Simplifying Mixed-Food Microwave Sample Preparation for ICP-MS Analysis
November 1st 2014Low-level analysis of food matrices has placed a demand on manufacturers, testing laboratories, and instrumentation vendors worldwide. Stricter regulations, better analytical instrumentation, and greatly improved sample preparation (preanalytical) techniques have focused efforts to simplify and standardize these analyses. Often overlooked, the preanalytical step determines the quality of the resulting data and requires careful attention to a number of details, including sample size, digestion parameters, and the level of detection needed.
Improving ICP-MS Analysis of Samples Containing High Levels of Total Dissolved Solids
November 1st 2014A novel approach to handling samples with very high and variable levels of sample matrix is to use aerosol dilution, whereby the amount of sample aerosol that reaches the plasma is reduced by dilution with an additional argon gas stream.
ICP Emission Spectrometry: Arsenic at 228 nm — Interferent or Analyte?
November 1st 2014This article compares several performance criteria such as full width at half maximum, background equivalent concentrations, limits of detection, purge requirements, and results for some substances for the "traditional" As lines at 188.979, 193.696, and 197.197 nm for the "new" line at 228.812 nm.