During a session at Analytica 2024 in Munich, Germany, experts from several universities and companies spoke about the latest trends in spectroscopy technology for a variety of applications. The session, which was chaired by Uwe Karst, a professor at the University of Münster, and Carsten Engelhard of Bundesanstalt für Materialforschung und -prüfung (BAM) & Universität Siegen (1).
The first part of the session began with “Mid-Infrared Arthroscopy: Real-Time In-Vivo Cartilage Condition,” presented by Boris Mizaikoff, a professor of chemistry at Ulm University and Director at the Hahn-Schickard Institute for Microanalysis Systems in Germany. Mizaikoff discussed sensing platforms that benefit from cascade lasers combined with miniaturized photonic platforms providing direct access to molecule-specific information, highlighting the utility of MIR catheter technologies for analyzing cartilage damage in-vivo during arthroscopic surgery, and discussed potential and challenges when translating this technology into clinical practice.
Mizaikoff was followed by Svenja Berit Seiffert, laboratory team leader at BASF in Germany and her discussion,“Advances in Quantitative Bioimaging of Nanomaterials using LA-ICP-MS: Implications for Nanotoxicology.” Recent research by Seiffert and associates includes laser ablation–inductively coupled plasma–mass spectrometry (LA-ICP-MS) being combined with immunohistochemical (IHC) staining with lanthanide-labeled antibodies to investigate the distribution of intratracheally instilled CeO2 NPs from the rat lung to lymph nodes, spleen, and liver (2).
Rene Boiteau of the University of Minnesota presented “Advancements in Environmental Metal Speciation Analysis by Multi Modal Mass Spectrometry.” Boiteau described recent advances in liquid chromatography mass spectrometry-based methods for separating, quantifying, and identifying the specific organic molecules that strongly bind metals in environmental samples, and discussed how our multi-modal approach has shed new light on the environment's chemical forms, sources, and transformations of metals.
This session concluded with Kerstin Leopold’s presentation “Advancing X-ray Fluorescence Spectrometry for (Trace) Element Determination in Biomedical Samples and Energy Materials.” Leopold, professor of analytical chemistry at the Institute for Analytical and Bioanalytical Chemistry (IABC) at Ulm University in Germany, presented the development and validation of a reliable method based on X-ray fluorescence spectrometry in total reflection set-up (TXRF) analysis for the accurate quantification of iron and other trace metals in a variety of biological samples, including spleen and liver cells, liver and placental tissues, and bone marrow-derived macrophages (3.4). The application of micro x-ray fluorescence μXRF for metal detection in various materials used in energy research, such as nanomaterials and polymer membranes for artificial photosynthesis, was also discussed (5,6).
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