Ion Chromatography Analysis of Bromate in Natural Water Samples Using Ammonia as a Preservative
Spectroscopy E-Books
Ethylenediamine, the preservative specified in EPA Method 300.1, can introduce a chromatographic artifact when analyzing samples containing elevated carbonate concentrations as a result of the formation of ethylenediamine carbamate. This artifact can compromise the ability to measure low levels of bromate in drinking water. The use of ammonia as an alternative preservative was investigated and found to produce improved bromate chromatography under challenging conditions. The improvement was seen on two different stationary phases, demonstrating that the benefit of this alternative preservative is independent of the column chemistry.
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Best of the Week: EAS Conference Coverage, IR Spectroscopy, Microplastics
November 22nd 2024Top articles published this week include highlights from the Eastern Analytical Symposium, a news article about the infrared (IR) spectroscopy market, and a couple of news articles recapping spectroscopic analysis of microplastics.
FT-IR Analysis of pH and Xylitol Driven Conformational Changes of Ovalbumin–Amide VI Band Study
November 21st 2024This study uses Fourier transform infrared (FT-IR) spectroscopy to analyze how the globular protein ovalbumin's secondary structures transition under varying pH conditions in the presence of the cosolvent xylitol, highlighting the role of noncovalent interactions in these conformational changes.
