Microwave Sample Prep for Heavy Metals Determination in Accordance with USP /
February 1st 2019Single reaction chamber (SRC) microwave digestion offers significant benefits over traditional microwave digestion for pharmaceutical samples: higher sample throughput, reduced labor and consumables costs, simplified workflow, and superior digestion quality.
Enhanced Protein Structural Characterization Using Microfluidic Modulation Spectroscopy
February 1st 2019This article introduces a new infrared (IR) technique, microfluidic modulation spectroscopy (MMS), that is designed to address these needs, and presents data from measurements of commercially available proteins. The data demonstrate significant increases in sensitivity, dynamic range, and utility for the determination of protein similarity (fingerprinting), quantitation, protein secondary structure, and protein stability and aggregation through thermal and chemical denaturation methods.
SEIRAS-optimized ATR Wafers for Interfacial Spectroelectrochemistry
February 1st 2019We show that a microgrooved ATR-SEIRAS optimized Si ATR wafer designed to allow high angles of incidence at the electrode-solution interface provides improved signal-to-noise in electrochemical ATR-SEIRAS.
Infrared Spectroscopy: New Frontiers Both Near and Far
Exploration of the chemistry of materials at micrometer and nanometer scales leads to a better macroscopic perspective, as illustrated here with examples from our ongoing research in materials, environmental, and biomedical applications