New developments in matrix-assisted laser desorption ionization (MALDI) technology enable decoupling of the ionization source from the time-of-flight mass analyzer for operation at atmospheric pressure (AP-MALDI). This technique also can be integrated with other types of mass analyzers, such as the ion trap.
A discovery-based, untargeted metabolomics analysis of hundreds of yeast metabolites under robust, controlled extraction conditions followed by identification is described.
Macro attenuated total reflection FT-IR spectroscopic imaging is a powerful and underutilized tool. This article presents an overview of approaches and opportunities for using this method to study dynamic processes such as diffusion, sorption, crystallization, and dissolution.
The authors describe a new method for making faster measurements of multidimensional NMR spectra. The technique involves acquiring a small number of projections and using them to reconstruct the entire spectrum.
Webinar Date/Time: Thursday, September 26, 2024 Morning Session: 10:00 AM EDT | 7:00 AM PDT | 3:00 PM BST | 4:00 PM CEST Afternoon Sesson: 12:30 PM EDT | 9:30 AM PDT | 5:30 PM BST | 6:30 PM CEST
The authors show that high resolution 1H nuclear magnetic resonance (NMR) spectroscopy can be used to study biofilm metabolism under environmentally relevant conditions in a minimally invasive way.
A look at the various strategies and tools related to metabolomics applied to food and nutrition.
IR and Raman spectroscopy are powerful analytical techniques to detect, discriminate and identify material on a molecular level. In particular Raman spectroscopy offers some advantages when applied to art and archaeology as well as earth sciences.
Recent developments in sample inlet systems, improved software, and the advent of special purpose mass spectrometers have improved the utility of MS instruments. here, the authors discuss this new utility.
We explain how to characterize barium fluorohalides with Raman spectroscopy.
This application note demonstrates the performance for the measurement of sulfur in ultra-low sulfur diesel using full polarization in 90° Cartesian geometry EDXRF.
The need for reference materials that can be applied in the area of thin films analysis has long been realized but is still, in general, under-addressed. Alumina films of single-micrometer thickness, having either fine distributions of impurities or delta function impurity marker layers, can be prepared routinely by anodic oxidation of electropolished aluminum specimens in appropriate electrolytes. Selected films were examined by transmission electron microscopy (TEM) and analyzed by radio frequency glow discharge optical emission spectroscopy (rf-GD-OES), providing very rapid, yet high-resolution, depth-resolved analysis of these electrically insulating materials.
BaySpec’s OCI-UAV hyperspectral imagers are ultra-compact, easily deployable, high-performance hyperspectral cameras designed specifically for use on small unmanned aerial vehicles (UAVs), to monitor the details of spatial, temporal, and spectral representation of ground objects.
This application note explores the characterization of graphene with an affordable modular Raman spectrometer system using the StellarNet HYPER-Nova.
Hydrophilic interaction liquid chromatography (HILIC) and reversed-phase high performance liquid chromatography (HPLC) are complementary techniques in the separation of organic molecules with a broad band of polarity. Both separation variants can be operated easily with volatile and water-miscible solvents (for example, ammonium acetate aqueous solution and acetonitrile). Thus, a hyphenation of both liquid chromatographic techniques with atmospheric pressure ionization (API) and mass spectrometry (MS) seems to be a consequent step.
The authors discuss progress in near-field IR microspectroscopy using a photothermal probe and show how it can be applied to the spectroscopic characterization of real-world samples.
A discovery-based, untargeted metabolomics analysis of hundreds of yeast metabolites under robust, controlled extraction conditions followed by identification is described.
ICP-OES can accurately measure the elemental ratios necessary to optimize battery performance and improve recycling efforts so that battery recoveries are optimized. The authors explore how ICP-OES can help manufacturers meet the increasing performance demands required for lithium-ion batteries.
The theme of the 2018 Eastern Analytical Symposium and Exposition is “Analytical Solutions to the World’s Problems.” The EAS has always been about problem solving. This year, we focus on problems that affect the world.
The method described here allows for the simultaneous analysis of 47 pesticides and five mycotoxins in cannabis in one simple QuEChERS procedure. This simple method is designed for implementation in start-up laboratories and in established laboratories that wish to streamline their sample preparation process, decrease solvent usage, and obtain accurate and fast results.
The analysis of amines by gas chromatograph ;mass spectrometry (GC–MS) using electron ionization (EI) has always been a challenge
The main limitations of quantification using MALDI imaging are discussed and the different approaches used for quantitative measurement in MSI are evaluated.
Through symposia, posters, and workshops, representatives from industry and academia addressed a broad range of technology and implementation issues that are beginning to change the landscape of modern spectroscopy.
This method demonstrates that ICP-OES is a suitable alternative to ICP-MS for the determination of rare earth elements in geological and agricultural samples
X-ray photoelectron spectroscopy (XPS) can be used to determine the contaminants present on laboratory gloves and to evaluate the type and amount of contamination transfer from gloves to other surfaces.
An update on the sample preparation and LC–MS-MS tools available for allergen detection, as well advantages of those techniques.