As this study demonstrates, energy-dispersive X-ray fluorescence (EDXRF) and multivariate statistical analysis can be used to distinguish different classes of historical artifacts, such as ancient pottery—revealing insights about theirs origin and uses.
A complex fluorescence method utilizing the Sn(II)-salicylfluorescein (SAF)-cetyltrimethylammonium bromide (CTMAB) system demonstrated effective detection of Sn(II) with a linear relationship between its concentration and fluorescence intensity, along with successful application in various sample matrices with high recovery rates.
We show how FT-IR may be used for quality control analysis of natrii sulfas, a transparent crystalline material used in natural medicine that primarily contains sodium sulfate decahydrate, crystallized from sulfate minerals.
Regulations have been imposed to set legal limits of nitrate and nitrite in water worldwide. In this study, a highly accurate and optimized ultraviolet (UV) spectroscopy method is proposed to simultaneously monitor nitrate and nitrite for rapid determination and continuous monitoring in environmental water applications.
A model has been developed to predict the “cold” or “hot” nature of Chinese medicines based on UV spectral data.
This study applied principal component regression (PCR) and partial least squares (PLS) algorithms for the spectrophotometric analysis of a drug containing antazoline hydrochloride (AN) and naphazoline hydrochloride (NP) without chemical separation. Both methods showed high accuracy and precision, with results closely matching those from a reference HPLC method, and were successfully validated for analyzing commercial pharmaceutical products.
The relationship between leaf nitrogen content (LNC) and hyperspectral remote sensing imagery (HYP) was determined to construct an estimation model of the LNC of drip-irrigated sugar beets, to enable real-time monitoring of sugar beet growth and nitrogen management in arid areas.
This article explains the key steps of using Raman technology to investigate carbon and carbon-based materials—such as carbon nanotubes, graphene, and carbon fibers and composites—as well as the process of analyzing the spectra.
An artificial neural network was combined with LIBS to provide a rapid and accurate coal-rock recognition method for unmanned coal mining.
A method combining inductively coupled plasma–mass spectrometry (ICP-MS) with inductively coupled plasma–optical emission spectrometry (ICP-OES) was developed for multielement determination of 50 species of major, minor, micro, and trace, rare earth, and rare elements in geological samples.
A rapid vis-NIR spectroscopy method for determining soil particle size and quality.
In this study, X-ray fluorescence (XRF) spectroscopy was used to analyze heavy metals in five traditional Mongolian medicines, and the results were compared to those obtained using ICP-MS.
We investigate the effect of an applied electric field on the laser-induced titanium plasma for laser induced breakdown spectroscopy (LIBS) for the purpose of assessing electron density with respect to laser energy.
In this study, a glycerol-fed, lab-scale E. coli bioprocess producing representative pharmaceutical compounds was monitored offline with a portable, high-sensitivity Raman spectrometer.
To study the optical properties of mixed crude oil, the optical constants of samples consisting of two crude oils mixed in different proportions were obtained by the double-thickness transmittance method based on transmittance spectra.
An inexpensive fiberoptic-based formaldehyde field sensor is described for monitoring low-levels of formaldehyde, a widespread indoor air pollutant, based on the principle of evanescent wave absorption of light. Sensor prototypes following that principle are being tested in two plywood board production plants.
The ICP–MS mass spectrum contains useful additional information, but how to obtain that information is the question. Here, we provide the answer.
This app note demonstrates the effectiveness of utilizing the NanoRam-1064 for analyzing and identifying botanical ingredients while minimizing fluorescence.
There is a growing desire among spectroscopists for having instruments small enough to be taken to the sample, as opposed to bringing the sample to the instrument. The result is that Raman spectrometers are becoming more miniaturized. Because these instruments come at a lower cost and offer distinct advantages over traditional spectrometers, the expectation is that a rapid expansion of when these instruments are applied will come forthwith. We offer a preview of how future miniaturized Raman spectrometers might look.
IR absorption spectroscopy technology can solve the problem of line aliasing in gas detection. Here, continuous wavelet transform was used in time-frequency analysis to improve spectral component identification and quantitative detection of gases.
Long chain fatty acids (LCFAs) function as a source of metabolic energy, substrates for membrane biogenesis, and storage of metabolic energy. Oxylipins, oxygenated derivatives of LCFAs, regulate the activity of many cellular processes. Existing methods for the analysis of LCFAs and oxylipins have limited compound coverage and sensitivity that, therefore, prevent their application in biological studies. In this work, we developed a high-throughput LC–MS method for analysis of 51 LCFAs and oxylipins. LCFAs and oxylipins were first extracted from biological samples via solid-phase extraction. The extracted molecules were analyzed by targeted comparative metabolomics. Saturated and monounsaturated LCFAs were analyzed in single ion reaction mode, while polyunsaturated LCFAs and oxylipins were analyzed in multiple reaction monitoring mode. Using this method, we successfully quantified 31 LCFAs and oxylipins from mouse livers.
This article discusses coherent Raman imaging and how it can visualize and quantify cutaneous pharmacokinetics (PK).
A deep learning model for predicting the size-dependent Raman shift of semiconductor nanomaterials was demonstrated and achieved via multi-layer perceptron.
The utility of the GladiATR diamond ATR, modified with an internal liquid light guide to illuminate the sample from underneath the ATR element, was explored to analyze the photo-polymerization of carbitol acrylate at 405 nm using 1 wt% TPO.
UV-Vis-NIR can be used to understand how ancient buildings were constructed. Here, a UV-Vis-NIR and EDXRF spectrophotometer were used to analyze glazed tiles that comprised a historical site built in Ancient China.
A deep learning model for predicting the size-dependent Raman shift of semiconductor nanomaterials was demonstrated and achieved via multi-layer perceptron.