An inexpensive fiberoptic-based formaldehyde field sensor is described for monitoring low-levels of formaldehyde, a widespread indoor air pollutant, based on the principle of evanescent wave absorption of light. Sensor prototypes following that principle are being tested in two plywood board production plants.
DNA effectively removes chrysene from contaminated water through intercalation, as confirmed by various analytical methods, offering a potential novel approach for chrysene elimination in water pollution.
The fast data acquisition and minimal sample preparation of handheld LIBS devices make them very useful for geochemical mapping, resource prospecting, sample selection, and hazard identification.
A review of exponential signal models with machine learning in nuclear magnetic resonance (NMR) spectroscopy is discussed here.
The implementation of 120 open-path spectroscopy analyzers at oil refineries has taught us lessons about compound identification, target species detectability, interferences, and data management, which can help spectroscopists generate more accurate data when monitoring air quality.
Inductively coupled plasma mass spectrometry (ICP-MS) instruments can perform low-level elemental analysis in a wide range of sample types, from high-purity chemicals to high matrix digests. But achieving consistently low detection limits requires good control of elemental contamination, as well as spectral interferences. A clean working area, careful selection of reagents, and good sample handling techniques are key to successful trace and ultratrace elemental analysis. In this article, we provide five practical tips for controlling contaminants and minimizing detection limits.
Nitrite poses health risks. This study evaluates the results of using tannic acid- protected fluorescence copper nanoclusters (TA-CuNCs) to detect nitrite in food.
Time-resolved fluorescence spectroscopy reveals much about the structure-induced energy transfer mechanisms of phycobilisomes, the light-harvesting antenna in cyanobacteria.
FT-IR offers an alternative method for the quantification and classification of lignocellulose in biofuel pellets, based on determination of cellulose, hemicellulose, and lignin content. The IR spectroscopic evaluation presented here provides an understanding of the pretreatment and storage of biofuel pellets.
This study applied principal component regression (PCR) and partial least squares (PLS) algorithms for the spectrophotometric analysis of a drug containing antazoline hydrochloride (AN) and naphazoline hydrochloride (NP) without chemical separation. Both methods showed high accuracy and precision, with results closely matching those from a reference HPLC method, and were successfully validated for analyzing commercial pharmaceutical products.
ATR-FT-IR spectroscopy can provide rapid and portable measurements in forensic applications, demonstrating its ability to rapidly detect biomarkers and the presence of cocaine in fingernails.
Graphene exhibits special properties, such as high strength and high electrical and thermal conductivity and as such is highly desirable for key electronic components. A new Raman spectroscopy sampling technique has been applied to the characterization of batches of graphene that provides a simple, at-line method for obtaining key product data.
Key Issues: Sampling flexibility of Raman enables in-process analysis of solids, turbid media, liquids, and gases Large volumetric Raman provide representative sampling of heterogenous solids
This study examines the fluorescence enhancement effects of forsythoside E, one of metabolites of Forsythia suspensa, on human serum albumin (HSA) and bovine serum albumin (BSA) under simulated physiological conditions.
In this study, the nitrophenol isomers, in solid and liquid phases, were analyzed using Raman spectroscopy, laying the groundwork for determining nitrophenol isomers in environmental monitoring with this technique.
Portable X-ray fluorescence was used to analyze the archaeological remains of an Underground Railroad station to gain a clearer understanding of the construction phases it underwent during the 19th century.
Perovskites are known to be useful for fabrication of solar cells, and their crystalline structure plays an important role in their electronic properties. Here, we show how Raman analysis is able to confirm the presence of the required crystalline phase for solar cell production.
As an alternative drug delivery route, transdermal patches control the amount of medication a patient receives. With confocal Raman microscopy it is possible to create a Raman 3D map and thus visualize and analyze the layers of a transdermal patch without damaging it, allowing for quality control and stability measurements.
Time-resolved fluorescence spectroscopy reveals much about the structure-induced energy transfer mechanisms of phycobilisomes, the light-harvesting antenna in cyanobacteria.
Is ICP-MS instrumentation ready to handle the requirements of AOAC Method 2015.01 for the determination of toxic elements in food—including dealing with interferences? We ran this study to check.
A celebration of the 36-year career of Ulrich J. Krull, on the occasion of his retirement earlier this year.
Spectroscopic ellipsometry, correlated with UV-vis-NIR spectroscopy, is used to determine the optical constants of thin films, such as in GexSb40-xSe60 chalcogenide glass.
Key Issues: Sampling flexibility of Raman enables in-process analysis of solids, turbid media, liquids, and gases Large volumetric Raman provide representative sampling of heterogenous solids
In combination with attenuated total reflectance (ATR), Fourier transform infrared (FT-IR) spectroscopy can be used to classify different moss species.
A model has been developed to predict the “cold” or “hot” nature of Chinese medicines based on UV spectral data.
To improve the robustness and accuracy of logistic regression identification method, a new Raman spectroscopy identification method was proposed that combines a distributionally robust optimization technique and fused lasso technique with logistic regression. Then, Raman spectroscopy was used to analyze two types of dairy products that were collected for anti-jamming identification testing to verify the effectiveness of the new method.